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Safe investigation design and data critique

Learning objectives

  • Outcome

    List at least three hazards in a given procedure and state a control for each.

  • Outcome

    Identify the independent, dependent, and controlled variables in an experiment description.

  • Outcome

    Calculate the mean of a measurement series and flag an outlier using the criterion ∣xi−xˉ∣>2s|x_i-\bar{x}|>2s.

  • Outcome

    Draft a safe investigation plan stating repetitions, units, and a risk-reduction method.

Understand the idea

Text

Safe investigation design starts from a testable hypothesis and a plan in which every measured quantity is tied to the question. Before measuring, identify hazards (electricity, hot surfaces, chemicals, lasers, heavy loads) and replace or isolate them; if a hazard cannot be removed, use a simulation. The design must explicitly state the independent variable xx that you change, the dependent variable yy that you measure, and the controlled variables that stay constant. For reliability, plan repetitions, randomization, and blind procedures where possible; record the instrument uncertainty Δx\Delta x and the units. Critiquing data requires checking calibration, units, outliers, and systematic errors, not only the mean xˉ\bar{x}. A conclusion is justified only if the data are reproducible and alternative explanations have been tested.

Worked examples

Direct

Problem

A student plans to heat 100 mL of water in a glass beaker on a hot plate and record the temperature every minute. List three hazards and a control for each. Identify the independent variable, dependent variable, and two controlled variables.

Solution

Hazards: the hot plate can cause burns; the glass beaker can break and cut; water spilled near an electrical socket can cause shock. Controls: use heat-resistant gloves and tongs; inspect the glass for cracks and use a heatproof mat; keep sockets away and keep hands dry. Independent variable: heating time tt (min). Dependent variable: water temperature TT (°C). Controlled variables: initial water volume V=100V=100 mL and initial water temperature T0T_0.

Application

Problem

Six repeated current measurements at a fixed voltage are 0.50, 0.51, 0.49, 0.52, 0.53, and 1.50 A. Calculate the mean and the sample standard deviation ss. Flag any outlier using ∣xi−xˉ∣>2s|x_i-\bar{x}|>2s. Then state one safety action and one data-critique action before repeating.

Solution

Sum the values: 0.50+0.51+0.49+0.52+0.53+1.50=4.050.50+0.51+0.49+0.52+0.53+1.50=4.05 A, so xˉ=4.05/6=0.675\bar{x}=4.05/6=0.675 A. Deviations from the mean are −0.175,−0.165,−0.185,−0.155,−0.145,0.825-0.175,-0.165,-0.185,-0.155,-0.145,0.825 A. The squared deviations sum to 0.817750.81775 A$^2$. The sample variance is s2=0.81775/5=0.16355s^2=0.81775/5=0.16355 A$^2$, so s≈0.404s \approx 0.404 A and 2s≈0.8092s \approx 0.809 A. For the last value, ∣1.50−0.675∣=0.825>0.809|1.50-0.675|=0.825 > 0.809, so it is flagged as an outlier. Safety action: check the circuit for a short or an overheated component before touching it. Data-critique action: verify the meter range and lead contact, then repeat the measurement; if the outlier persists, record it and investigate the cause rather than deleting it.

Transfer

Problem

You want to test whether the rate of a chemical reaction increases with acid concentration. The reaction produces hydrogen gas and uses a strong acid. Design a safe investigation or simulation. State variables, controls, repetitions, units, and one data-critique rule.

Solution

Safe design: use a simulation of reaction rate versus concentration; if physical work is necessary, use dilute acetic acid and a small magnesium ribbon, safety goggles, ventilation, and no open flame because of hydrogen. Variables: independent — acid concentration cc (mol/L); dependent — gas production rate (mL/s) or time to collect 20 mL of gas. Controls: temperature TT, magnesium mass mm, surface area, acid volume. Repetitions: 3 trials for each concentration. Data-critique rule: plot rate versus cc; flag outliers with ∣xi−xˉ∣>2s|x_i-\bar{x}|>2s; check the gas syringe calibration; reject data if a leak is suspected. Conclude only if the trend is reproducible and monotonic.

Practice

Text

Use a free circuit simulation (for example, PhET Ohm’s Law). Choose a fixed resistor and vary the voltage from 0 to 5 V in steps of 0.5 V, recording the current. Then deliberately insert one incorrect value into the table. Before starting, list the hazards of a real circuit (short circuit, burn, overheating) and explain why the simulation is used. Take at least six repeated current measurements at one voltage: for n=3n=3 the maximum possible deviation from the mean is 2s/3≈1.155s2s/\sqrt{3}\approx 1.155s, so the criterion ∣xi−xˉ∣>2s|x_i-\bar{x}|>2s can never flag an outlier, whereas for n≥6n\ge 6 the criterion works. Calculate the mean current and flag any outlier using ∣xi−xˉ∣>2s|x_i-\bar{x}|>2s. Write 5 sentences of critique: units, calibration, repetitions, outlier, possible systematic error.

Visual reference

Purpose

Show how hypothesis, hazard check, variables, procedure, data, and the decision to conclude or redesign are connected.

Representation

Flowchart: “Hypothesis” → “Hazard check” → “Variables (xx, yy, controls)” → “Safe procedure or simulation” → “Data table” → “Check units and calibration” → “Outlier and uncertainty” → “Conclude or redesign”.

Real-world examples

Ruler-drop reaction time: sport and safe experiment

Scenario

A student tests whether light warm-up improves reaction. A partner holds a 3030 cm ruler so its lower edge is level with the thumb and releases it without warning; the student catches it with the same hand. Before and after 55 minutes of warm-up they record 1010 trials each. Safety: warm-up without running through the lab, the ruler falls away from the face, and there are no bags around to trip over. For a fall distance d=0,18d=0{,}18 m the reaction time is t=2d/g=2⋅0,18/9,8≈0,19t=\sqrt{2d/g}=\sqrt{2\cdot0{,}18/9{,}8}\approx0{,}19 s; for d=0,25d=0{,}25 m it becomes ≈0,23\approx0{,}23 s.

Connection

This tests safe design: controlled drop height, one hand, the same partner, no obstacles. Data critique is needed to notice an outlier: one trial with d=0,32d=0{,}32 m gives t≈0,26t\approx0{,}26 s and is probably caused by distraction; it must not be silently averaged in. Repeats and spread show random error.

Bicycle braking distance on dry and wet asphalt

Scenario

A cyclist of mass 6060 kg rides along a marked straight at 1515 km/h =4,17=4{,}17 m/s and brakes with only the front brake to a full stop. On dry asphalt three braking distances are 3,13{,}1, 3,03{,}0, 3,23{,}2 m; on wet asphalt they are 4,84{,}8, 6,26{,}2, 5,15{,}1 m. Safety: helmet, closed area without cars, a 1010 m wet patch, speed no higher than 1515 km/h, and walking the bicycle back after each braking. Means: dry 3,13{,}1 m, wet 5,45{,}4 m.

Connection

The scenario uses risk assessment and control of variables: the same tyres, pressure, mass and speed. Data critique requires comparing repeats and explaining the outlier 6,26{,}2 m — perhaps the puddle is deeper; without repeats the conclusion 'wet is always 1,71{,}7 times longer' would be unjustified. The spread gives the uncertainty of the mean.

Boiling salted water: kitchen, thermometer, and outlier

Scenario

In a kitchen they test whether salt changes the boiling point. In 250250 ml of water at 101101 kPa they boil pure water, then add 1010 g of table salt and bring it to boiling again. The thermometer is fixed so that it does not touch the bottom. Pure water: 100,0100{,}0 °C; with salt: 100,5100{,}5 °C, 101,2101{,}2 °C, 100,6100{,}6 °C. Safety: goggles, a glove for hot cookware, the stove cord away from water, and no tasting of the solution.

Connection

This is safe design: fixed volume, pressure, thermometer position, and burn protection. Data critique reveals a systematic error: if the thermometer touches the bottom, it reads 103103 °C, and that is not the boiling point. The reading 101,2101{,}2 °C is checked by repeating the measurement; the mean of the two agreeing values is ≈100,55\approx100{,}55 °C.